Advances in Carbohydrate Chemistry and Biochemistry, Vol. 7 by Sidney M. Cantor

By Sidney M. Cantor

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4-Methyl-~-fructose.. . . . . . . . . . . . . . . . . . . B-Methyl-~-fructose.. . . . . . . . . . . . . . . . . . . . . . 5-Methyl-D,cfructose (1) . . . . . . . . . . . . . . . . . XII. Trityl Ethers.. . . . . . . . ...................

J. DIMLER carbon atom 1the configuration opposite that of the terminal asymmetric carbon atom 5, as in the 8-D-glucopyranosides. The complete structure assigned to the glucosan, therefore, was D-glucosan < 1,4>/3 < 1,6> or 1,6-anhydro-~-~-glucofuranose (11). 111. D-GALACTOSAN < 1,4> a < 1,6> 1. Preparation The pyrolytic vacuum distillation of D-galactose was investigated by Hann and HudsonKrelative to the formation of levogalactosan, D-galactosan < 1,5>8 < 1,6> . They found that a dextrorotatory D-galactosan was formed along with levogalactosan.

28 R. A. LAIDLAW AND E. Q. V. PERCIYAL TABLEI The Methyl Ethers of D-Xylose Subs1ance 2-Methyl-~-xylose -, -, anilide 3,&diacetate -, triacetate -, 3,4-di-p-toluenesulfonate -, methyl 8-D-pyranoside '&Methyl-D-xylonic acid, -, lactone Melting point, "C. I D I . ) +46 +30 HzO 15 +23 - -30+ -26 -82 +22 - 16 77 15 - 15 17 0 H2 12 CHClr 14 Dioxane 17 Hi0 EtOH (77) R. A. 5. Bywater, W. N. Haworth, E. L. Hirst and 5. Peat, J . Chem. , 1983 (1937). ) HzO 14, 78 -+ (78) H. D. K. Drew, E. H. Goodyear and W.

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