Chemical Engineering Kinetics (Mcgraw-Hill Chemical by J. M. Smith

By J. M. Smith

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Extra resources for Chemical Engineering Kinetics (Mcgraw-Hill Chemical Engineering Series)

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I'OH 107b - 107a - CbHgLi 8% 38 9% 14% Substances Derived from Chrysanthemic Acid 39 Sucrow and Richter's synthesis of the Chrgtien-Bessisre monoterpene (Z)lz7 is illustrated in Scheme 11,13' and Sucrow's Scheme 11 H3C\ /CH3 C -CH -CH =C\ H3C/ IOH CH2 I CH3 I 1. H202 ___c 2. 140 The principal of the two syntheses is practically the same as for the same author's earlier santolinatriene synthesis (see above). -CH=CHOCH3 H5C202C'IOH 1. LiAlH4 2. H ~ O + c *In Scheme 12, the alcohol (E) is acetylated (to before proceeding with the lithium t-butoxyaluminm hydride reduction.

9 8 ) . 28 The S y n t h e s i s of Monoterpenes i n f l u e n c e of a c i d c a t a l y s t s * ) . C i t r a l can be made from g e r a n i o l (21) by many v a r i e t i e s of o x i d a t i o n procedure ( s e e R e f . 103, f o r a l i s t , t o g e t h e r with many o t h e r s y n t h e s e s ) , b u t p a r t i c u l a r l y potassium dichromate i n a c e t i c a c i d , which a f t e r r e f l w i n g f o r 1 h r , t h e n steam d i s t i l l i n g , i s r e p o r t e d l b 4 t o g i v e almost q u a n t i t a t i v e y i e l d s .

66 - 64 - 65 - Isopulegol Citronella1 41b Citral b 41a 68 - Citral a Isocitral _. 1 67 a-Citronella1 Ci tral e) Both n a t u r a l and s y n t h e t i c c i t r a l i s a mixture of t h e two poss i b l e isomeric forms, c i t r a l a ( = g e r a n i a l , and c i t r a l b (=neral, The two isomers have been w e l l c h a r a c t e r i z e d by NMR a n a l y s i s , l o ' l o 2 and i n t h e commonly encountered mixt u r e s t h e trans- form ( g e r a n i a l , +) i s g e n e r a l l y t h e predominating isomer.

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