By Michael B. Smith
The Compendium of natural man made Methods serves as a convenient laptop reference for natural chemists to browse new reactions and changes of curiosity, facilitating the hunt for practical staff modifications within the unique literature of natural chemistry. quantity thirteen includes either useful staff adjustments and carbon-carbon bond forming reactions from the literature within the years 2005-8. It offers examples of released reactions for the training of monofunctional compounds.
The Compendium of natural man made tools sequence allows the quest for caliber, chosen practical team alterations, equipped through reacting useful staff of beginning fabric and useful workforce shaped, with complete references to every reaction
Presents examples of released reactions for the instruction of monofunctional compounds from the literature of 2005-8
Provides a convenient reference and a precious device to the operating natural chemist, permitting a brief payment of identified natural transformations
Stringent standards for inclusion of reactions, together with genuine artificial application of reactions, reagents on hand or simply ready and dealt with within the laboratory
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Extra info for Compendium of Organic Synthetic Methods
Kotani ,S. ; Ishizuka , T. ; Hashimoto ,S . Tetrahedron Lett. 2005, 46,157 . C. ; Gamsey ,S. ; Knueppel , D. ;Steiner , D. ; DeLaTorre ,K. ; Singaram ,B . Tetrahedron Lett. 2005, 46, 2315 . - J . - M . -S . Tetrahedron Lett. 2005, 46, 2695 . - C . - L . - P . Tetrahedron Lett. 2005, 46, 4573 . - C . - L . - P . Tetrahedron Lett. 2005, 46, 6209 . ,CHO PhB(OH) 2, Et 2 Zn, toluen e BINOL typ eligand s Ito, K. ; Tomita , Y. ; Katsuki ,T . Tetrahedron Lett. 2005, 46, 6083 . Ph quant (88 %ee ) 36 Compendiumo f Organi cSyntheti c Methods ,Vo l1 3 BfOI- n' Section 34 B OH -Et 2Zn, toluen e, 60° C, 12 h 2.
Gevorgyan , V . J. Am. Chem. Soc. 2007, 129, 7742 . For example so f th e reactio n RC=C H - > R O C - O C R (Alkyne- A lkyne) . SECTION 12: A, o 1 "Ph ,se eSectio n 30 0 ALKYNES FROM KETONES PCl5«xPy ,21 0se c microwaves, 110°C ; the nHC 1 =P h 74 % MeP h Ghaffarzadeh, M. ; Bolourtchian , M. H. R. ; Mohsenzadeh ,F . Synth. Commun. 2006, 36,1973 . SECTION 13: ALKYNES FROM NITRILES % Compendiumo f Organi cSyntheti c Methods ,Vo l1 3 10 Section1 5 NO ADDITIONA L EXAMPLE S SECTION 14: ALKYNES FROM ALKENES H =—Si(/- P r) Ph 3.
2006, 71,804 . ,OTf cat. M O ( C O ) 6, H 2 0, microwave s M e 'Me Lesma, G. ; Sacchetti , A. ;Silvani ,A . Synthesis 2006,594 . 4 N C S ,MeC N, 10° C PhSAc PhS0 2 Cl 2M HCl- M eC N Nishiguchi, A. ; Maeda ,K. ;Miki ,S . Synthesis 2006, 4131 . PhCH 2 C0 2 Me ,C02H cat. 4) ,37° C 72°, ' 96% PhCH 2 C0 2 H 99% Barbayianni,E. ; Fotakopoulou ,I. ; Schmidt ,M. ; Constantinou- K okotou , V. ; Kokotos, G . J. Org. Chem. 2005, 70, 8730 . Other reaction s usefu l fo r th e hydrolysi so f ester sma yb e foun di nSectio n30 A (Protection o f Carboxyli cAci dDerivatives) .